/ Home
/ SUBMISSION

/ The BJOC
/ Diamond Open Access
/ Journal Statistics
/ Editorial Board
/ Community
/ Call for papers

/ Latest Articles
/ Most accessed
/ Thematic issues
/ Volumes
/ Authors

/ Alerts

/ TWITTER
/ LINKEDIN
/ Mastodon
/ RSS FEED

Empty search

Article Type

Publication Date Range

Search Tips

This search combines search strings from the content search (i.e. "Full Text", "Author", "Title", "Abstract", or "Keywords") with "Article Type" and "Publication Date Range" using the AND operator.

Search Examples

aromatic	the word “aromatic”
aromatic aldehyde	the word “aromatic” OR “aldehyde”
+aromatic +aldehyde	both words “aromatic” AND “aldehyde”
+aromatic -aldehyde	the word “aromatic” but NOT “aldehyde”
“aromatic aldehyde”	the exact phrase “aromatic aldehyde”
benz*	words which begin with “benz”, such as “benzene” or “benzyl”
benz*yl	words that begin with “benz” and end with “yl”, such as “benzyl” or “benzoyl”
benzyl~	words that are close to the word “benzyl”, such as “benzoyl” (i.e., fuzzy search)

BROWSE
Latest Articles
Most accessed
thematic issues
volumes
authors

BROWSE

Latest Articles Most Accessed Thematic Issues Volumes Authors

Author

1 article(s) from Otth, Elisabeth

Synthesis, characterization and initial evaluation of 5-nitro-1-(trifluoromethyl)-3H-1λ³,2-benziodaoxol-3-one

Nico Santschi,
Roman C. Sarott,
Elisabeth Otth,
Reinhard Kissner and
Antonio Togni

Beilstein J. Org. Chem. 2014, 10, 1–6, doi:10.3762/bjoc.10.1

PDF

Graphical Abstract

Figure 1: Electrophilic trifluoromethylating agents 1 and 2.

Jump to Figure 1

Scheme 1: Synthesis of 5-nitro-1-(trifluoromethyl)-3H-1λ³,2-benziodaoxol-3-one (3).

Jump to Scheme 1

Figure 2: UV–vis spectra of reagents 2 (green) and 3 (blue) in DMSO/H₂O 1:1.

Jump to Figure 2

Figure 3: ORTEP representation of X-ray structures 6 and 3. Thermal ellipsoids set to 30% probability. Hydrog...

Jump to Figure 3

Figure 4: DSC traces obtained for 2 (green) and 3 (blue).

Jump to Figure 4

Figure 5: Cyclic voltammetry of 3 (1 mM, black) and of a mixture of 3 (1 mM) and methyl 2-iodo-5-nitrobenzoat...

Jump to Figure 5

Figure 6: Sample kinetic traces for the decomposition of 2 (green) and 3 (blue) to 4 and 5, respectively, upo...

Jump to Figure 6

Album

Supp Info

Full Research Paper

Published 02 Jan 2014

Full text

Other Beilstein-Institut Open Science Activities

/ Help / Support & Contact / Alerts / Privacy Policy / Terms & Conditions / Impressum

Synthesis, characterization and initial evaluation of 5-nitro-1-(trifluoromethyl)-3H-1λ3,2-benziodaoxol-3-one

Synthesis, characterization and initial evaluation of 5-nitro-1-(trifluoromethyl)-3H-1λ³,2-benziodaoxol-3-one